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Article overview
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Heat treatment - microstructure - hardness relationships of new nickel-rich nickel-titanium-hafnium alloys developed for tribological applications | Sean H. Mills
; Christopher Dellacorte
; Ronald D. Noebe
; Michael J. Mills
; Aaron P. Stebner
; Behnam Amin-Ahmadi
; | Date: |
17 Sep 2020 | Abstract: | The effects of various heat treatments on the microstructure and hardness of
new Ni56Ti41Hf3 and Ni56Ti36Hf8 (atomic %) alloys were studied to evaluate the
suitability of these materials for tribological applications. A solid-solution
strengthening effect due to Hf atoms was observed for the solution annealed
(SA) Ni56Ti36Hf8 alloy (716 HV), resulting in a comparable hardness to the
Ni56Ti41Hf3 alloy containing 54 vol.% of Ni4Ti3 precipitates (707 HV). In the
Ni56Ti41Hf3 alloy, the maximum hardness (752 HV), achieved after aging at 300C
for 12 h, was attributed to dense, semi-coherent precipitation of the Ni4Ti3
phase. Unlike the lenticular morphology usually observed within binary NiTi
alloys, a blocky Ni4Ti3 morphology formed within Ni56Ti36Hf3 due to a smaller
lattice mismatch in the direction normal to the habit plane at the
precipitate/matrix interface. The maximum hardness for Ni56Ti36Hf8 (769 HV) was
obtained after applying an intermediate aging step (300C for 12 h) followed by
normal aging (550C for 4 h). This two-step aging treatment induces dense
nanoscale precipitation of two interspersed precipitate phases, namely H-phase
and a new cubic Ni-rich precipitate phase, resulting in the highest hardness
exhibited yet by this family alloys. The composition of cubic Ni-rich
precipitates was measured using atom probe tomography to be approximately
Ni61.5Ti31Hf7.5, while HAADF-STEM revealed a 54 atom motif cubic structure (a=
8.87 Angstroms), and electron diffraction showed that the structure belongs to
the pm-3m (No. 221) space group. | Source: | arXiv, 2009.07962 | Services: | Forum | Review | PDF | Favorites |
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